Solubility - preferred solvent:
DMSO
Solubility - concentration:
10 mM
NMR:
1H NMR (500 MHz, CD2Cl2, TMS) δ 7.41 (d, J = 8.5 Hz, 1 H, 4-H), 7.28 (d, J = 8.5 Hz, 1 H, 5-H), 7.17 (t, J = 10.7 Hz, 1 H, 2′-H), 4.46-4.41 (m, 2 H, NH2), 4.41 (q, J = 7.1 Hz, 2 H, CH2), 4.38 (s, 3 H, 1-CH3), 1.44 (t, J = 7.1 Hz, 3 H, CH2CH3);
13C NMR (125 MHz, CD2Cl2, TMS) δ 161.6 (C=O), 146.9 (C-2′), 135.5 (C-7a), 131.1 (C-6), 130.2 (C-2), 126.5 (C-3a), 123.5 (C-5), 121.6 (CN), 120.6 (C-4), 116.9 (C-7), 112.3 (C-3), 74.9 (C-1′), 62.2 (CH2), 35.6 (1-CH3), 14.3 (CH2CH3);
Chemical Probes Portal KH-CB19.pdf
