NMR:
1H NMR (500 MHz, (CD3)2SO) δ ppm 8.15 (s, 1H), 8.03−7.98 (m, 1H), 7.98−7.94
(m, 1H), 7.91 (s, 1H), 7.82−7.76 (m, 2H), 6.76 (br.s, 2H), 4.10 (q, J =
7.0, 2H), 3.64−3.57 (m, 1H), 3.21−3.12 (m, 2H), 3.10−3.00 (m, 2H),
2.06−1.96 (m, 2H), 1.96−1.85 (m, 2H), 1.32 (t, J = 7.0, 3H); 13C NMR
(125 MHz, (CD3)2SO) δ ppm 157.6, 149.7, 147.7, 142.2, 137.5, 134.1,
131.9, 130.7, 130.5, 130.3 (q, JC−F = 31.7), 125.0 (q, JC−F = 3.7), 124.60
(q, JC−F = 3.7), 124.59 (q, JC−F = 272.6), 123.1, 114.4, 49.9, 49.0, 44.0,
30.6, 15.2; 19FNMR(376 MHz, (CD3)2SO) δ ppm −61.0
Chemical Probes Portal I-BRD9.pdf
