Solubility - concentration:
>439 uM
NMR:
1H NMR (DMSO-d6 ,600MHz): δ = 11.37 (br d, J = 2.0 Hz, 1H), 8.44 (d, J = 1.5 Hz, 1H), 8.35 (d, J = 2.0 Hz, 1H), 7.67 (s, 1H), 7.60 (s, 1H), 7.54 (d, J = 1.3Hz, 1H), 6.82 (br d, J = 8.4 Hz, 1H), 4.34 (br s, 1H), 3.36 (br dd, J = 9.5, 5.9 Hz, 2H), 3.26 (s, 3H), 3.20 - 3.25 (m, 1H, ), 3.07 - 3.19 (m, 4H), 2.38 (s, 3H), 2.23 - 2.28 (m, 1H), 2.22 (br d, J = 2.4 Hz, 1H), 2.08 (d, J = 0.9 Hz, 3H), 1.68 (dt, J = 6.6, 3.4 Hz, 2H), 1.40 - 1.58 (m, 2H), 1.29 - 1.40 (m, 3H), 0.71 - 0.90 (m, 2H).
13C NMR (151 MHz, DMSO-d6) δ = 162.0, 148.5, 147.3, 147.0, 139.0, 137.4, 134.0, 132.9, 132.9, 132.0, 124.1 (t, J = 240 Hz), 120.9, 120.1, 117.6, 80.0 (2C), 73.7, 58.0, 57.3, 49.4, 49.0, 35.2, 32.3 (2C, t, J = 30 Hz), 25.0 (2C), 17.9, 16.7.
19F NMR (376 MHz, DMSO-d6) δ = -89.3 (d, J = 233 Hz, 1F), -99.5 (ddd, J = 233, 33, 9 Hz, 1F).
